1• Objectives of the training, expected outcomes and review of the agenda.
2• Principles of spectroscopy.
3 • Principles & operation of AAS.
Laboratory session
4. Learning components of AAS, i.e. Assembling the sample introduction system.
5 • AAS gas requirements.
6 • Consumables and spares.
7 • Introduction to AAS technique, Basic Principle, its Applications and Uses in various fields.
8.Sample preparation techniques.
9.Wet digestion.
10• Dry ashing Fusion.
11• Microwave assisted digestion.
12.Laboratory session.
Laboratory session
13• Preparation of organic sample.
14.Preparation of inorganic samples.
15• Preparation of difficult samples.
16• Software basic and instrument set-up.
17. Calibration curve.
18 • Use of quality control.
19.• Internal QCs – spiking, HRM, replicate testing.
20• External QCs – CRM, PTs, ILC.Laboratory session
21• Preparation of standards
22.Preparation of QCs
23• Method development
24• Sample analysis using AAS
25• Introduction and Hands-on practice on preparation of different types of samples for determination of heavy metals
26• Hands-on practice on preparation of different types of samples for determination of heavy metals.
27• Analysis of different types of food sample.
Laboratory session
28• Analysis of different types of food sample.
29• Analysis of different types of water sample.
30• Analysis of data & uncertainty measurements.
31• Maintenance of AAS and Trouble-shooting covering all the possible problems.
32• Course overview.
33.Conclusion.
2• Principles of spectroscopy.
3 • Principles & operation of AAS.
Laboratory session
4. Learning components of AAS, i.e. Assembling the sample introduction system.
5 • AAS gas requirements.
6 • Consumables and spares.
7 • Introduction to AAS technique, Basic Principle, its Applications and Uses in various fields.
8.Sample preparation techniques.
9.Wet digestion.
10• Dry ashing Fusion.
11• Microwave assisted digestion.
12.Laboratory session.
Laboratory session
13• Preparation of organic sample.
14.Preparation of inorganic samples.
15• Preparation of difficult samples.
16• Software basic and instrument set-up.
17. Calibration curve.
18 • Use of quality control.
19.• Internal QCs – spiking, HRM, replicate testing.
20• External QCs – CRM, PTs, ILC.Laboratory session
21• Preparation of standards
22.Preparation of QCs
23• Method development
24• Sample analysis using AAS
25• Introduction and Hands-on practice on preparation of different types of samples for determination of heavy metals
26• Hands-on practice on preparation of different types of samples for determination of heavy metals.
27• Analysis of different types of food sample.
Laboratory session
28• Analysis of different types of food sample.
29• Analysis of different types of water sample.
30• Analysis of data & uncertainty measurements.
31• Maintenance of AAS and Trouble-shooting covering all the possible problems.
32• Course overview.
33.Conclusion.
